www.graceinstrument.com

Products
Applications
Datasheets
Download
Trainings
Supports
Knowledge Bank
 

Laboratory Viscometer Application Data Sheet

Oil / Gas Well Drilling Fluids

Application

Drilling for oil and gas requires sensitive viscosity instrumentation, especially at low-shear rates, to insure that production is optimized. Field viscosity measurements on drilling and fracturing fluids are required to predict flow performance under the extremely low shear conditions applicable to solids transport down hole. Grace Instrument Company's Programmable M3500 and M5500 Viscometer provides sensitive, low-shear rate viscosity (LSRV) measurements and is rapidly becoming the instrument of choice when Oil/Gas service companies need to verify performance of expensive fracturing fluids and drilling muds immediately prior to use.  

Required Equipment

For analyzing drilling fluid rheological properties in the field, Grace Instrument Company's M3500 Viscometer used with the API standard rotors and bobs provides the complete solution for LSRV measurement under a variety of tough field conditions.

Test Method

Having chosen one of the rotor and bob geometries mentioned above in Required Equipment, the procedure involves running a test at two or more different rotational speeds. The objective is to run at a very low speed between 0.01 and 0.1 rpm and a second rotational speed between 1.0 and 6.0 rpm. These speeds would generally equate to shear rates below 0.1 sec-1 and 10 sec-1 respectively. If the instrument has sufficient viscosity measurement range, a higher speed test at 600 rpm can also be considered.
On tests run by a field service company on three different fracturing fluids, the following values were obtained:

Shear Rate Fluid A (cP) Fluid B (cP) Fluid C (cP)
5.11 sec-1 800 780 900
1,400 27,000 2,500


The above values show that the three different fluids would exhibit very similar viscosity behavior at shear rates around 3254 sec-1 and higher, but drastically different viscosity values at the lower shear rate of 0.0027 sec-1. In order to suspend particles down hole, the higher viscosity value at very low shear rate is important; therefore, Fluid B is a much better solution for the application.

Options

A more detailed test can be created using Grace Instrument Company's WingatherTM software which provides automatic data collection. In addition, the software will calculate yield point and plastic viscosity by using the appropriate mathematical model which is included in the software.

Higher shear rate measurements can be made if appropriate. The Grace Instrument Company M3500 Viscometer is capable of measuring shear rates up to 3254 sec-1. The Grace Instrument Company M5500 viscometer can measure up to and beyond 1870 sec-1 with the sample pressurized up to 1000 psi. For making measurements at low shear rates under pressurized conditions, please refer to Grace Instrument Company Application, "Oil/Gas Exploration and Drilling".

 

Oil / Gas Exploration And Drilling

Application

Field engineers on-site at oil and gas drilling wells need to perform rapid viscosity tests which simulate pressurized process conditions for down-hole environments. Applications include fracturing fluids, drilling muds, cements and oil/water emulsions, all at elevated temperatures characteristic of down-hole conditions. The M5500 viscometer is an ideal replacement for the standard Fann® Model 50 viscometers and Nordman viscometers which are bulky, expensive, and cumbersome to operate.

Problem Description

Field engineers in oil and gas drilling operations can make a serious financial mistake (perhaps as much as $500,000) if the viscosity specifications of fluids pumped down-hole are incorrect. This complicates testing procedures, increases the risk of costly errors and wastes time. Consequently, it's necessary to ensure fast, accurate viscosity measurement, data collection and analysis of small fluid samples (tested under pressure and elevated temperatures) before they are pumped down-hole.

Solution

The portable M5500 viscometer gives field engineers reliable viscosity measurement on-site at the well, simplifies complicated test procedures, minimizes human error and ensures quality control without delay. The Grace Instrument Company M5500 bench-top viscometer:

  • Permits easy relocation to the most remote job site due to its small size and light weight
  • Allows quick and easy viscosity measurements under pressure and elevated temperature
  • Provides complete automation of standard test procedures and conditions
  • Obtains real-time data collection and analysis at multiple shear rates
  • Utilizes coaxial cylinder geometry identical to existing standards
  • Allows easy cleaning and disassembly due to simple, straightforward design
  • Isolates torque transducer, bearings and other mechanisms from sample/test environment
  • Minimum vapor space above sample
  • More sensitive than competitive instruments

Companies Involved In Oil/Gas Exploration And Drilling


Major Oil/Gas field service companies

  • Oil/Gas companies
  • Oil/Gas well owners
  • Technical labs/consultants
  • Suppliers of fluids used in Oil/Gas well development
  • Qualifying Your Application

Do you need to measure fluid samples under multiple shear conditions and at elevated pressure and/or temperature?
Are you already using an expensive, large-size viscometer?
Or do you use atmospheric "standard" (Model Fann® 35) viscometers because the large size and weight of other instruments restricts you from taking the instrument to remote well sites?
Do you need to rapidly move a pressurizable viscometer from one remote location to another?
Are you building a new mobile test van/truck where the size and weight of the instrumentation needs to be small enough to fit inside?
If you answer "yes" to any of the above questions, then the M5500 is a good solution for your requirements.

Benefits

Prevents very costly mistakes in the field by insuring that all fracturing fluids, drilling muds, and cements meet viscosity specifications before being pumped down-hole
Reduces the risk of procedural errors attributable to operator haste
Compact size, light weight and portability quickly allow the M5500 viscometer to be set up rapidly and perform real-time tests on multiple samples in virtually any location, even the most remote job site
Complete software package included in base price, eliminating the need for further development to make the system operational
Less susceptible to dust compared to other field instruments
Choice of cylinder geometry allows duplication of standard test methods
Better sensitivity allows measurement at much lower shear rates than previously available


Model 5500 HTHP Viscometer Specifications

Dimensions:

8.5" x 12.5" x 24" (with bath)

 

Weight:

   

37 lbs (with bath)

 

Construction:

316 Stainless Steel (Hastelloy C available)

 

Pressure Range:

   

Vacuum to 1000 psi

 

Temperature Range:

32~500 degree Fahrenheit (°F)

 

Speed Range:

   

0.0001~1100 rpm continuous

 

Sample Size:

13~43 ml

 

Shear Rate Range:

   

0.00004~1870 sec-1

 

Resolution:

0.01% of full scale range or better

 

Repeatability:

   

±0.05% of full scale range

 

Computer:

PC with Pentium processor

 

Voltage:

   

115V or 230V (with transformer)

 

Frequency:

50 Hz or 60 Hz


References


The American Petroleum Institute (API) has recommended standard procedures for three key areas in Oil/Gas exploration/drilling where the M5500 viscometer could be used: fracturing fluids, drilling muds and cements. These procedures require special speeds over defined time periods and temperatures. The references below include these standard procedures:

  1. Recommended Practice on the Rheology and Hydraulics of Oil-Well Drilling Fluids. API Recommended Practice 13D, 3rd Edition, June 1, 1995
  2. Recommended Practice Standard for Laboratory Testing Drilling Fluids. API Recommended Practice 13I, 5th Edition, June 1, 1995
  3. Recommended Practice Standard Procedure for Field Testing Oil-Based Drilling Fluids. API Recommended Practice 13B-2 (RP 13B-2), 2nd Edition, December 1, 1991
  4. Practice Standard Procedure for Field Testing Water-Based Drilling Fluids. API Recommended Practice 13B-1 (RP 13B-1), 1st Edition, June 1, 1990
  5. Recommended Practices on Measuring the Viscous Properties of a Cross-linked Water-based Fracturing Fluid. API Recommended Practice 39 (RP 39), 3rd Edition, May 1998

 

* Fann® is the registered trade mark of Fann Instrument Company

 






Email

     © 2005 Grace Instrument Company. All rights reserved.